Methyl butyrate → (cis,trans)-1,4-Cyclohexanedicarboxaldehyde

HRID 991397ノート

反応式

HRID 991397 の反応式
[CH3:1][CH2:2][CH2:3][C:4]([O:6]C)=O>C(CC=O)CC=O>[CH:3]1([CH:4]=[O:6])[CH2:2][CH2:1][CH:3]([CH:4]=[O:6])[CH2:2][CH2:1]1

参加物

3

反応物 1

HCID 12180Methyl butyrate

生成物 1

HCID 10154096(cis,trans)-1,4-Cyclohexanedicarboxaldehyde

試薬・触媒・溶媒 1

HCID 3485Glutaraldehyde溶媒

実験手順

The procedure according to Example 17 was repeated, but using the same amount of the polymer obtained from Example 10 instead of the polymer obtained from Example 1; 1,4-cyclohexane dicarboxaldehyde (1.4 g) as a cross-linker instead of glutaric dialdehyde, and methyl 3-methylpropionate (25 ml) as a solvent, to obtain a negative pattern with a resolution of 0.15 μm (FIG. 3).

出典と根拠

ORDレコード
ord-17ad5e1751fc420a8e670d8bef2beea1
出典データセット
uspto-grants-2002_10
特許番号
US06465147B1

反応ノート

読み込み中…