Acetic Acid → 1-iodo-2,3-dimethoxybenzene
반응식
CO[C:3]1[CH:4]=[C:5]([CH:7]=[C:8]([O:10][CH3:11])[CH:9]=1)N.N([O-])=O.[Na+].Cl.[I-:17].[K+].[C:19]([OH:22])(=O)C>>[CH3:11][O:10][C:8]1[C:7]([O:22][CH3:19])=[C:5]([I:17])[CH:4]=[CH:3][CH:9]=1참가 물질
6
실험 절차
converting 3,5-dimethoxyaniline into a diazonium salt thereof with using sodium nitrite in acetic acid in the presence of a hydrochloric acid, and reacting the product with potassium iodide to give dimethoxyiodobenzene;
출처 및 근거
- ORD 기록
- ord-e817abf4cc5c4384aa110159b18ed604
- 출처 데이터셋
- uspto-grants-2000_04
- 특허 번호
- US06048842
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