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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1004438생성일: 2026년 10월 26일

Potassium Acetate → Benzenemethanol, 3,5-bis(1,1-dimethylethyl)-4-hydroxy-, 1-acetate

https://huagongshe.com/reaction/1004438

반응식

참여 물질

역할이름HCID투입량
반응물Potassium AcetateHCID 517044—
반응물2,6-Di-tert-butyl-4-(chloromethyl)phenolHCID 12378601—
용매AcetoneHCID 180—
생성물Benzenemethanol, 3,5-bis(1,1-dimethylethyl)-4-hydroxy-, 1-acetateHCID 8440445%

반응 조건

온도20 °C

반응 단계

A mixture of 4-chloromethyl-2,6-di-t-butylphenol (2.55 g) and potassium acetate (0.98 g) in acetone (30 mL) was stirred at 20° C. for 24 hours. After evaporation of the solvent the residue was partioned between water and n-hexane. The hexane extract was concentrated and the residue slurried in n-hexane (6 mL) at about 0° C. The crystals were collected via filtration and dried to give 1.54 g, 45% yield, of the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06048995
출처 데이터셋uspto-grants-2000_04
ORD IDord-c9941dd45f3945949a83a9d18e02784d
출처 메모uspto-grants-2000_04