反应详情

温度

20 °C

A mixture of 4-chloromethyl-2,6-di-t-butylphenol (2.55 g) and potassium acetate (0.98 g) in acetone (30 mL) was stirred at 20° C. for 24 hours. After evaporation of the solvent the residue was partioned between water and n-hexane. The hexane extract was concentrated and the residue slurried in n-hexane (6 mL) at about 0° C. The crystals were collected via filtration and dried to give 1.54 g, 45% yield, of the title compound.

1. customAfter evaporation of the solvent the residue
2. extractionThe hexane extract
3. concentrationwas concentrated
4. customslurried in n-hexane (6 mL) at about 0° C
5. filtrationThe crystals were collected via filtration
6. customdried
7. customto give 1.54 g, 45% yield