Sodium borohydride → HCID 18791153, 화합물

HRID 1005348

반응식

HRID 1005348 반응식
[Cl:1][C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[S:7][C:6]=2[C:5]([O:17][CH2:18][CH2:19][CH3:20])=[CH:4][CH:3]=1.[BH4-].[Na+]>CO>[Cl:1][C:2]1[C:15]2[CH:14]([OH:16])[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[S:7][C:6]=2[C:5]([O:17][CH2:18][CH2:19][CH3:20])=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 4311764Sodium borohydrideHCID 52128569H-Thioxanthen-9-one, 1-chloro-4-propoxy-

생성물 1

HCID 18791153HCID 18791153, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

1-Chloro-4-propoxy-9H-thioxanthen-9-one (20 g, 65.6 mmol) was reduced with sodium borohydride (6.5 g, 0.17 mol) in methanol (320 ml) and worked up following the procedure described in Example 22(i) to give the title compound as a white solid.

출처 및 근거

ORD 기록
ord-90f7ade9f8324d909462b3bb2ca3511b
출처 데이터셋
uspto-grants-2000_04
특허 번호
US06054448

연결된 노트

불러오는 중…