4-Chloro-2-methyl-6-nitroaniline → HCID 22668925, 화합물

HRID 1007230

반응식

HRID 1007230 반응식
[Cl:1][C:2]1[CH:8]=[C:7]([N+:9]([O-:11])=[O:10])[C:5]([NH2:6])=[C:4]([CH3:12])[CH:3]=1.[Cl:13][C:14]1[CH:22]=[CH:21][C:17]([C:18](Cl)=[O:19])=[CH:16][N:15]=1>>[Cl:13][C:14]1[N:15]=[CH:16][C:17]([C:18]([NH:6][C:5]2[C:4]([CH3:12])=[CH:3][C:2]([Cl:1])=[CH:8][C:7]=2[N+:9]([O-:11])=[O:10])=[O:19])=[CH:21][CH:22]=1

참가 물질

3

반응물 2

HCID 1823554-Chloro-2-methyl-6-nitroanilineHCID 27821656-Chloronicotinoyl Chloride

생성물 1

HCID 22668925HCID 22668925, 화합물

실험 절차

The title compound was prepared from 4-chloro-2-methyl-6-nitroaniline (204 mg, 1.09 mmol) and 6-chloronicotinoyl chloride (192 mg, 1.09 mmol) and obtained as a light yellow solid as described in Example 62. 1H NMR (CDCl3): 9.13 (s, 1H), 8.96 (dd, J=0.6, 2.4 Hz, 1H), 8.20 (dd, J=2.7, 8.4 Hz, 1H), 7.93 (d, J=2.4 Hz, 1H), 7.59 (d, J=2.4 Hz, 1H), 7.51 (dd, J=0.6, 8.1 Hz, 1H), 2.38 (s, 3H).

후처리

  1. customobtained as a light yellow solid

출처 및 근거

ORD 기록
ord-ec54ddd7cc5543d6b06139b5a426c519
출처 데이터셋
uspto-grants-2004_09
특허 번호
US06794397B2

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