Hydrochloric Acid → HCID 54402950, 화합물

HRID 1010522노트

반응식

HRID 1010522 반응식
C([O:3][C:4](=[O:13])[CH2:5][N:6]1[CH:10]=[C:9]([CH2:11][CH3:12])[N:8]=[CH:7]1)C.Cl>>[CH2:11]([C:9]1[N:8]=[CH:7][N:6]([CH2:5][C:4]([OH:13])=[O:3])[CH:10]=1)[CH3:12]

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 57731307HCID 57731307, 화합물

생성물 1

HCID 54402950HCID 54402950, 화합물

실험 절차

1.7 g (9.5 mmol) of (4-ethyl-imidazol-1-yl)-acetic acid ethyl ester are dissolved in 47 ml (190 mmol) 4N HCl and the mixture is heated to reflux. After 2 h the mixture is cooled to rt and the solvent is removed in vacuo. The resulting product is used without further purification.

후처리

  1. temperaturethe mixture is heated to reflux
  2. customthe solvent is removed in vacuo
  3. customThe resulting product is used without further purification

출처 및 근거

ORD 기록
ord-bb57c63f9b0d41b99bff4471bff17847
출처 데이터셋
uspto-grants-2011_07
특허 번호
US07977323B2

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