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Ammonia → 2,6-Lutidine

HRID 1012370
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HRID 1012370 반응식
N.[BH3:2].C([N:5]([CH2:12][CH3:13])[C:6]1[CH:11]=[CH:10][CH:9]=C[CH:7]=1)C.B.[C:15]1([N:21]2[CH2:26][CH2:25][O:24][CH2:23][CH2:22]2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.B.[N:28]1C(C)=CC=CC=1C>>[C:15]1([N:21]2[CH2:26][CH2:25][O:24][CH2:23][CH2:22]2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[N:5]1[C:6]([CH3:7])=[CH:11][CH:10]=[CH:9][C:12]=1[CH3:13].[NH3:28].[BH3:2]
참가 물질실험 절차출처 및 근거반응 노트

참가 물질

7

반응물 4

HCID 222Ammonia2회HCID 83312Diethylaniline-boraneHCID 15265529(T-4)-Trihydro(4-phenylmorpholine-kappaN4)boronHCID 178419164HCID 178419164, 화합물

생성물 3

HCID 79372,6-LutidineHCID 623394-PhenylmorpholineHCID 419330
Ammonia;borane

실험 절차

For example, dimethylaniline borane can be reacted with ammonia to produce ammonia borane as shown below. (C6H5)(CH3)2N.BH3+NH3=(C6H5)(CH3)2N+NH3.BH3 In other examples, diethylaniline borane, phenylmorpholine borane or lutidine borane can be reacted with ammonia to form ditethylaniline and ammonia borane, phenylmorpholine and ammonia borane, or lutidine and ammonia borane.

출처 및 근거

ORD 기록
ord-889a1419970e4c178f8797f81dee20b9
출처 데이터셋
uspto-grants-2011_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07977508B2

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