Calcium Carbonate → Tricalcium Phosphate

HRID 1027325

반응식

HRID 1027325 반응식
[OH:1][P:2]([O-:5])([O-:4])=[O:3].[Ca+2:6].C(=O)([O-])[O-].[Ca+2]>[Pt].O>[O-:3][P:2]([O-:5])([O-:4])=[O:1].[O-:3][P:2]([O-:5])([O-:4])=[O:1].[Ca+2:6].[Ca+2:6].[Ca+2:6]

참가 물질

5

반응물 2

HCID 10112Calcium CarbonateHCID 24441Calcium hydrogen phosphate

생성물 1

HCID 24456Tricalcium Phosphate

시약·촉매·용매 2

HCID 23939Platinum촉매2회HCID 962Water용매

반응 조건

온도
1400 °C

실험 절차

For a mixture of 500 g (dry weight), 360 g dicalcium phosphate anhydrous powder, 144 g calcium carbonate powder and 220 ml deionized water were mixed for 7 minutes at 500 rpm using a laboratory stirrer. The slurry from the mixing process was immediately transferred into a high temperature stable platinum cup. The filled platinum cup was placed in a cold furnace. The furnace was heated to 1400° C. by using a heating rate of 60° C. per hour. The heating process was stopped after 72 hours by switching off the furnace. The sample was cooled down to room temperature within the furnace. The bulk sintered material (phase pure α-Ca3(PO4)2) was removed from the furnace and the platinum cup. The bulk product from the sintering process had a weight of 420 g (weight loss 16.7%).

후처리

  1. additionwere mixed for 7 minutes at 500 rpm
  2. temperatureThe sample was cooled down to room temperature within the furnace
  3. customThe bulk sintered material (phase pure α-Ca3(PO4)2) was removed from the furnace

출처 및 근거

ORD 기록
ord-5abea6d7314748ff8c651ae508a1e199
출처 데이터셋
uspto-grants-2014_05
특허 번호
US08734524B2

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