Sodium Hydroxide → 2-(Ethylhydroxyphosphinyl)acetic acid sodium salt

HRID 1028264노트

반응식

[CH2:1]([P:3]([OH:9])([CH2:5][C:6]([OH:8])=[O:7])=[O:4])[CH3:2].[OH-].[Na+:11]>>[Na+:11].[CH2:1]([P:3]([OH:9])([CH2:5][C:6]([O-:8])=[O:7])=[O:4])[CH3:2]

참가 물질

반응물 2

HCID 14798Sodium Hydroxide

HCID 15357685[Hydroxy(ethyl)phosphinyl]acetic acid

생성물 1

HCID 462412532-(Ethylhydroxyphosphinyl)acetic acid sodium salt수율 98%

실험 절차

An aqueous solution of 304 g (2 mol) of 2-(ethylhydroxyphosphinyl)acetic acid (produced according to Example 10) is reacted with about 160 g of a 50% strength aqueous solution of sodium hydroxide and the water is distilled off in vacuo to obtain 384 g (98% of theory) of 2-(ethylhydroxyphosphinyl)acetic acid sodium salt as colorless solid.

후처리

distillationthe water is distilled off in vacuo

출처 및 근거

ORD 기록: ord-c71b4e76b1ef4e2fa52c857a83b2ad0d
출처 데이터셋: uspto-grants-2014_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08735476B2

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