Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl p-toluenesulfonate → 5-Chloro-2-methylthio-3-methylbenzothiazolium tosylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl p-toluenesulfonate | HCID 6645 | — |
| 반응물 | 5-Chloro-2-(methylthio)benzothiazole | HCID 645746 | — |
| 생성물 | 5-Chloro-2-methylthio-3-methylbenzothiazolium tosylate | HCID 86745614 | — |
반응 단계
5-Chloro-2-(Methylthio)benzothiazole (5.0 g, 0.023 mol) and 4.40 g methyl p-toluenesulfonate were heated to 152° C. for 7 minutes. Upon cooling, the mixture solidified and then was triturated with acetone to give 7.82 g (84%), mp 170°-185° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05102781 |
| 출처 데이터셋 | uspto-grants-1992_04 |
| ORD ID | ord-ccf7747bc7e0489c849ed2b64f55902a |
| 출처 메모 | uspto-grants-1992_04 |