huagongshe.com
HRID1029359

反应详情

EQUATION

反应方程式

HRID 1029359 的结构方程式

REACTANTS

反应物

2
结构：COS(=O)(=O)c1ccc(C)cc1
HCID6645

Methyl toluene-4-sulfonate

C8H10O3S

结构：CSc1nc2cc(Cl)ccc2s1
HCID645746

5-Chloro-2-(methylthio)benzothiazole

C8H6ClNS2

PRODUCTS

生成物

1
结构：CSc1sc2ccc(Cl)cc2[n+]1C.Cc1ccc(S(=O)(=O)[O-])cc1
HCID86745614

未命名化合物

PROCEDURE

实验过程

5-Chloro-2-(Methylthio)benzothiazole (5.0 g, 0.023 mol) and 4.40 g methyl p-toluenesulfonate were heated to 152° C. for 7 minutes. Upon cooling, the mixture solidified and then was triturated with acetone to give 7.82 g (84%), mp 170°-185° C.

WORKUP

后处理

  1. temperatureUpon cooling
  2. customwas triturated with acetone
  3. customto give 7.82 g (84%), mp 170°-185° C.