Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triphenylphosphine → (5 Chlorobenzoxazol-2-yl methyl)triphenylphosphonium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | 2-(Bromomethyl)-5-chlorobenzo[d]oxazole | HCID 12745945 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | (5 Chlorobenzoxazol-2-yl methyl)triphenylphosphonium bromide | HCID 23055263 | — |
반응 단계
A solution of the bromide (500 mg) (Step 3) and triphenylphosphine (740 mg) in CH3CN (5 mL) was stirred at room temperature overnight. The reaction mixture was diluted with Et2O (20 mL), stirred for 30 min, and filtered to give the title compound as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04957932 |
| 출처 데이터셋 | uspto-grants-1990_09 |
| ORD ID | ord-07367f49a302496b9fb474ee9f3acff1 |
| 출처 메모 | uspto-grants-1990_09 |