Water → HCID 15057055, 화합물
반응식
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C([O-])([O-])=O.[K+].[K+].Cl[C:15]1[CH:20]=[CH:19][N:18]=[CH:17][C:16]=1[N+:21]([O-:23])=[O:22].O>CN(C=O)C>[N+:21]([C:16]1[CH:17]=[N:18][CH:19]=[CH:20][C:15]=1[O:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)([O-:23])=[O:22]참가 물질
6
실험 절차
To phenol (6.5 g) in 20 ml DMF at room temperature was added K2CO3 (20 g) and this mixture stirred for 15 minutes at room temperature. Then 4-chloro-3-nitropyridine (10.0 g) in 60 ml DMF was added dropwise and the mixture stirred for two hours at ambient temperature. The mixture was poured into water and extracted with ethyl acetate. The organic layer was washed with water and dried (sat. NaCl, anhy. MgSO4).
후처리
- stirringthe mixture stirred for two hours at ambient temperature
- extractionextracted with ethyl acetate
- washThe organic layer was washed with water
- dry with materialdried (sat. NaCl
출처 및 근거
- ORD 기록
- ord-17c964ed95c141f78522f65fdda6c718
- 출처 데이터셋
- uspto-grants-1990_09
- 특허 번호
- US04959377
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