Benzoic anhydride → Benzoic Acid

HRID 1032867

반응식

HRID 1032867 반응식
[C:1]([O:9]C(=O)C1C=CC=CC=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C1C2=C3C(=CC=C2)C=CC=C3C=1>C(#N)C>[C:1]([OH:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 7167Benzoic anhydride3회HCID 9161Acenaphthylene2회

생성물 1

HCID 243Benzoic Acid

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

All reactions were run on a 10 mL scale at room temperature for a total of 5.00 min. The benzoic anhydride and internal standard were added from a stock solution which was 1.0M benzoic anhydride and 25,000 pm acenaphthylene in 100% acetonitrile. A total of 5.0 μL of this stock was used (yielding a 1:2000 dilution) to make each reaction 0.5 mM benzoic anhydride and 25 ppm acenaphthylene. Benzoic acid produced was measured by HPLC (high pressure liquid chromatography) using the acenaphthylene internal standard as a reference.

후처리

  1. customwere run on a 10 mL scale at room temperature for a total of 5.00 min
  2. customyielding a 1:2000 dilution)

출처 및 근거

ORD 기록
ord-ff17610db45246418b847043e928669d
출처 데이터셋
uspto-grants-1994_05
특허 번호
US05308529

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