Hydrochloric Acid → 1H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

HRID 1033747노트

반응식

HRID 1033747 반응식
[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][N:2]1C(OCC)=O.[ClH:15]>>[ClH:15].[ClH:15].[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][NH:2]1

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 18953633ethyl 1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylate

생성물 1

HCID 189536441H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

실험 절차

10.4 g (51 mmol) of ethyl 2,3-dihydro-1H-pyrrolo-[3,4-c]pyridine-2-carboxylate are refluxed for 15 hours together with 100 ml of concentrated hydrochloric acid. The batch is evaporated, and the crystalline residue is stirred with acetone. The product is filtered off with suction and dried in the air.

후처리

  1. customThe batch is evaporated
  2. filtrationThe product is filtered off with suction
  3. customdried in the air

출처 및 근거

ORD 기록
ord-da275ca293f44d51a9ea56983ed6266b
출처 데이터셋
uspto-grants-1994_05
특허 번호
US05312823

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