3-(4-Chlorophenyl)-1-(1,1-dimethylethyl)-1H-pyrazolo(3,4-d)pyrimidin-4-amine → Lytron 810

HRID 1033821

반응식

HRID 1033821 반응식
CC(N1N=[C:8]([C:10]2[CH:15]=[CH:14][C:13](Cl)=[CH:12][CH:11]=2)[C:7]2C(N)=NC=NC1=2)(C)C.[C:22]1(=[O:28])[O:27][C:25](=[O:26])[CH:24]=[CH:23]1.C=CC1C=CC=CC=1.C=CC.C(OOC(C1C=CC=C(C(OOC(C)(C)C)(C)C)C=1)(C)C)(C)(C)C>>[C:25]1(=[O:26])[O:27][C:22](=[O:28])[CH:23]=[CH:24]1.[CH2:7]=[CH:8][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

참가 물질

6

실험 절차

A thermoplastic resin composition was produced in the same manner as in Example 40, except that in place of MS-PP-2 and MS-EPM-2, a co-grafting product of the starting polypropylene for MS-PP-2 and the starting ethylene-propylene copolymer rubber for MS-EPM-2 was used. In a Hensachel mixer, 100 parts by weight of a blend of powder of the starting polypropylene for MS-PP-2 and pellets of the starting ethylene-propylene copolymer rubber for MS-EPM-2 in the ratio of 55:23 was uniformly mixed with 1.5 parts by weight of maleic anhydride, 0.5 part by weight of styrene, 0.6 part by weight of the propylene homopolymer containing as free-radical initiator 8% by weight of 1,3-bis(t-butylperoxyisopropyl)benzene (Sanperox®-TY1.3, mfd. by Sanken Kako Co., Ltd.) supported thereon, and 0.1 part by weight of 1010 (mfd. by Ciba-Geigy Ltd.) as stabilizer. The resulting mixture was melt-kneaded by means of a TEX 44 SS-30BW-2V type twin screw extruder mfd. by JAPAN STEEL WORKS, LTD., at a temperature of 220° C. for an average residence time of 1.5 minutes to obtain a (maleic anhydride-styrene)-co-grafted polypropylene/ethylene-propylene copolymer rubber having an amount of maleic anhydride added of 0.24% by weight, an amount of styrene added of 0.23% by weight and a melt flow rate of 15 g/10 min. This co-grafting product is hereinafter abbreviated as MS-(PP-2/EPM-2).

출처 및 근거

ORD 기록
ord-6f409fa0cdae48e1bc390a7fff4ea7a7
출처 데이터셋
uspto-grants-1994_05
특허 번호
US05312867

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