Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl p-toluate → HCID 19023272, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl p-toluate | HCID 66743 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | N-Cyclohexyl-N,4-dimethylbenzenesulfonamide | HCID 614169 | — |
| 생성물 | HCID 19023272 | HCID 19023272 | 90.1% |
반응 단계
Utilising the procedure described in Example 1(a) employing N-cyclohexyl-N-methyl 4-methylbenzenesulphonamide (20.0 g, 0.075 mol) in lieu of ethyl 4-methylbenzoate and two equivalents of NBS (27.0 g, 0.15 mol) yielded a crude product of N-cyclohexyl-N-methyl 4-bromomethylbenzenesulphonamide (23.4 g, 90%) as an orange oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05314880 |
| 출처 데이터셋 | uspto-grants-1994_05 |
| ORD ID | ord-bdb763b948854923a02d346864ef977a |
| 출처 메모 | uspto-grants-1994_05 |