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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1039062생성일: 2026년 10월 26일

5-nitro-2-(1H-1,2,4-triazol-1-yl)pyridine → 6-(1H-1,2,4-triazol-1-yl)pyridin-3-amine

https://huagongshe.com/reaction/1039062

반응식

참여 물질

역할이름HCID투입량
반응물5-nitro-2-(1H-1,2,4-triazol-1-yl)pyridineHCID 2766764—
촉매PalladiumHCID 23938—
용매MethanolHCID 887—
생성물6-(1H-1,2,4-triazol-1-yl)pyridin-3-amineHCID 16772327—

반응 단계

5-nitro-2-(1H-1,2,4-triazol-1-yl)pyridine (100 mg, 0.523 mmol) from step 1 of this example was added Pd/C (111 mg, 0.105 mmol) and methanol (5.2 mL). Set the reaction on Parr Shaker at 50 psi (345 kPa) for overnight. The solution was filtered through CELITE and rinsed with methanol to give the title compound as a white solid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08552022B2
출처 데이터셋uspto-grants-2013_10
ORD IDord-fbe714709af342a7b7b3c79361752d35
출처 메모uspto-grants-2013_10