Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → HCID 178477595, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | HCID 178477596 | HCID 178477596 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | HCID 178477595 | HCID 178477595 | — |
반응 단계
To a solution of benzyl (5S)-1-oxo-2-{trans-4-[(triethylsilyl)oxy]cyclohexyl}-2,7-diazaspiro[4.5]decane-7-carboxylate (2.4 g, 0.0048 mol) in methanol (10 mL, 0.2 mol) was added Pd/C, and the suspension was stirred at rt under a H2 balloon for 1.5 h. The inorganics were filtered and the filtrate was concentrated to afford the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08563570B2 |
| 출처 데이터셋 | uspto-grants-2013_10 |
| ORD ID | ord-da8bca61678646aeb0250b4a9ab7955f |
| 출처 메모 | uspto-grants-2013_10 |