3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenyl acetate → 3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenol
반응식
C([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([C:11]2[N:15]=[C:14]([CH3:16])[O:13][N:12]=2)[CH:6]=1)(=O)C>Cl>[CH3:16][C:14]1[O:13][N:12]=[C:11]([C:7]2[CH:6]=[C:5]([OH:4])[CH:10]=[CH:9][CH:8]=2)[N:15]=1참가 물질
3
실험 절차
A solution of 8.55 g (39.18 mmol) of the product obtained in Step C above in 120 ml of 1N HCl solution is heated at reflux for 90 minutes and is then left at ambient temperature overnight, with stirring. The precipitate is filtered off to yield the title product.
후처리
- temperatureat reflux for 90 minutes
- filtrationThe precipitate is filtered off
출처 및 근거
- ORD 기록
- ord-10a488ae5abf4fc5897e9468539c7837
- 출처 데이터셋
- uspto-grants-2013_10
- 특허 번호
- US08569285B2
반응 노트
불러오는 중…