Sodium Azide → Diisobutyl aluminium azide

HRID 1047654

반응식

HRID 1047654 반응식
[N-:1]=[N+:2]=[N-:3].[Na+].[Cl-].[CH2:6]([Al+:10][CH2:11][CH:12]([CH3:14])[CH3:13])[CH:7]([CH3:9])[CH3:8]>C1(C)C=CC=CC=1>[N-:1]=[N+:2]=[N-:3].[CH2:6]([Al+:10][CH2:11][CH:12]([CH3:14])[CH3:13])[CH:7]([CH3:9])[CH3:8]

참가 물질

4

반응물 2

HCID 33557Sodium AzideHCID 16686353Diisobutyl aluminium chloride

생성물 1

HCID 86610998Diisobutyl aluminium azide

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

1.235 g of granular sodium azide (19 mmol) are added to a cold solution of diisobutyl aluminium chloride (19 mmol, 1.8M in toluene) diluted in 5 ml of toluene and the mixture is stirred at room temperature over the night to give diisobutyl aluminium azide.

출처 및 근거

ORD 기록
ord-64e4130e48684bdfb9deb439bc89815c
출처 데이터셋
uspto-grants-2013_10
특허 번호
US08569528B2

연결된 노트

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