Calcium chloride, dihydrate → Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate
반응식
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH:3]([C:8]([O-:10])=[O:9])[CH:2]2[C:11]([O-:13])=[O:12].[Na+].[Na+].O.O.[Cl-].[Ca+2:19].[Cl-]>O>[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH:3]([C:8]([O-:10])=[O:9])[CH:2]2[C:11]([O-:13])=[O:12].[Ca+2:19]참가 물질
4
반응 조건
- 온도
- 60 °C
실험 절차
To a solution of disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate (22.6 g, 0.1 mol) in water (150 g) was added a solution of calcium chloride dihydrate (14.7 g, 0.1 mol) in water (100 g). The mixture stirred at 60° C. for 2 hours. The resulting white precipitate was filtered. The white powdery product was dried and milled (m.p. >300° C.).
후처리
- filtrationThe resulting white precipitate was filtered
- customThe white powdery product was dried
- custommilled (m.p. >300° C.)
출처 및 근거
- ORD 기록
- ord-c0156d75e2c14a898911d22916c87e2d
- 출처 데이터셋
- uspto-grants-2006_08
- 특허 번호
- US07094820B2
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