Iodine → HCID 87410566, 화합물
반응식
[CH2:1]([C:3]1[C:16]2[NH:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[S:8][C:7]=2[CH:6]=[CH:5][CH:4]=1)[CH3:2].[I:17]I>C(Cl)(Cl)Cl>[I-:17].[CH2:1]([C:3]1[C:16]2[C:7](=[S+:8][C:9]3[C:14]([N:15]=2)=[CH:13][CH:12]=[CH:11][CH:10]=3)[CH:6]=[CH:5][CH:4]=1)[CH3:2]참가 물질
4
반응 조건
- 온도
- 0 °C
실험 절차
1-Ethyl-10H-phenothiazine (646 mg, 2.84 mmol) was dissolved in CHCl3 (10 mL) and cooled to 0° C. as a solution of Iodine (2.16 g, 8.51 mmol) dissolved in CHCl3 (50 mL) was added dropwise. The mixture was stirred at 0° C. for 2 h, then allowed to warm to RT overnight.
후처리
- additionwas added dropwise
- temperatureto warm to RT overnight
출처 및 근거
- ORD 기록
- ord-c0839109fa6644149ac231e8e11bfdf7
- 출처 데이터셋
- uspto-grants-2016_07
- 특허 번호
- US09382221B2
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