Tetraethyltin → HCID 68628549, 화합물

반응식

[CH2:1]([O:5][C:6]([C:8]1[N:13]=[C:12](Br)[C:11]2[C:15]([CH3:18])=[N:16][S:17][C:10]=2[C:9]=1[OH:19])=[O:7])[CH2:2][CH2:3][CH3:4].[CH2:20]([Sn](CC)(CC)CC)[CH3:21]>>[CH2:1]([O:5][C:6]([C:8]1[N:13]=[C:12]([CH2:20][CH3:21])[C:11]2[C:15]([CH3:18])=[N:16][S:17][C:10]=2[C:9]=1[OH:19])=[O:7])[CH2:2][CH2:3][CH3:4]

참가 물질

반응물 2

HCID 11704Tetraethyltin

HCID 86649354HCID 86649354, 화합물

생성물 1

HCID 68628549HCID 68628549, 화합물

실험 절차

The title compound was synthesized in analogy to Example 28 from 4-bromo-7-hydroxy-3-methyl-isothiazolo[4,5-c]pyridine-6-carboxylic acid butyl ester and tetraethyltin: MS (m/z) 295.2 (M+1).

출처 및 근거

ORD 기록: ord-105ef514d8f94f5bb57655a5ad6a94ac
출처 데이터셋: uspto-grants-2016_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09387200B2

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