Phenol → 4-Bromo-N-methyl-2-nitro-3-phenoxyaniline

HRID 1057020노트

반응식

HRID 1057020 반응식
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1F.[C:14]1([OH:20])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1[O:20][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

참가 물질

3

반응물 2

HCID 996PhenolHCID 1180938324-Bromo-3-fluoro-N-methyl-2-nitroaniline

생성물 1

HCID 1180939434-Bromo-N-methyl-2-nitro-3-phenoxyaniline

실험 절차

This compound was synthesized according to the procedure of Example 1, Step 1, using 4-bromo-3-fluoro-N-methyl-2-nitroaniline and phenol as the starting materials. LCMS calculated for C13H12BrN2O3 (M+H)+: m/z=323.0, 325.0. found: 322.9, 325.0.

후처리

  1. customThis compound was synthesized

출처 및 근거

ORD 기록
ord-c1a0929503084d6a83700e700684d8be
출처 데이터셋
uspto-grants-2016_07
특허 번호
US09399640B2

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