Acetic Anhydride → N-(3-bromo-4-methoxyphenyl)acetamide

HRID 1059183

반응식

HRID 1059183 반응식
[Br:1][C:2]1[CH:7]=[C:6]([N+:8]([O-])=O)[CH:5]=[CH:4][C:3]=1[O:11][CH3:12].[C:13](OC(=O)C)(=[O:15])[CH3:14]>[Fe]>[Br:1][C:2]1[CH:7]=[C:6]([NH:8][C:13](=[O:15])[CH3:14])[CH:5]=[CH:4][C:3]=1[O:11][CH3:12]

참가 물질

4

반응물 2

HCID 7918Acetic AnhydrideHCID 788702-Bromo-4-nitroanisole

생성물 1

HCID 244158N-(3-bromo-4-methoxyphenyl)acetamide

시약·촉매·용매 1

HCID 23925Iron촉매

실험 절차

By the reaction in the same manner as in Example 33-(i) using 2-bromo-4-nitroanisole (5.41 g), iron powder (6.49 g) and acetic anhydride (4.4 ml), the title compound (4.87 g) was obtained as a colorless powder crystals.

출처 및 근거

ORD 기록
ord-86b40695a4af4a518e8fd0c57262b5ed
출처 데이터셋
uspto-grants-2003_02
특허 번호
US06518257B1

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