Thionyl Chloride → 3-Ethylbenzoyl chloride

HRID 1062644

반응식

HRID 1062644 반응식
[CH2:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6](O)=[O:7])[CH3:2].S(Cl)([Cl:14])=O>CN(C)C=O>[CH2:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6]([Cl:14])=[O:7])[CH3:2]

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 96207Benzoic acid, 3-ethyl-

생성물 1

HCID 128093233-Ethylbenzoyl chloride

시약·촉매·용매 1

HCID 6228Dimethylformamide촉매

실험 절차

3-Ethylbenzoic acid (9.40 g, 62.6 mmol) was added slowly to thionyl chloride (45 mL) at 0° C., and N,N-dimethylformamide (3 drops) was added dropwise. The obtained reaction mixture was refluxed under heating as it was for 2 h. The reaction mixture was concentrated and used without purification in the next reaction.

후처리

  1. customThe obtained reaction mixture
  2. temperaturewas refluxed
  3. temperatureunder heating as it
  4. concentrationThe reaction mixture was concentrated
  5. customused without purification in the next reaction

출처 및 근거

ORD 기록
ord-d2a2341ea8204d60af313ec6cefd3139
출처 데이터셋
uspto-grants-2005_11
특허 번호
US06962933B1

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