Thionyl Chloride → 3-Ethylbenzoyl chloride
반응식
[CH2:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6](O)=[O:7])[CH3:2].S(Cl)([Cl:14])=O>CN(C)C=O>[CH2:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6]([Cl:14])=[O:7])[CH3:2]참가 물질
4
실험 절차
3-Ethylbenzoic acid (9.40 g, 62.6 mmol) was added slowly to thionyl chloride (45 mL) at 0° C., and N,N-dimethylformamide (3 drops) was added dropwise. The obtained reaction mixture was refluxed under heating as it was for 2 h. The reaction mixture was concentrated and used without purification in the next reaction.
후처리
- customThe obtained reaction mixture
- temperaturewas refluxed
- temperatureunder heating as it
- concentrationThe reaction mixture was concentrated
- customused without purification in the next reaction
출처 및 근거
- ORD 기록
- ord-d2a2341ea8204d60af313ec6cefd3139
- 출처 데이터셋
- uspto-grants-2005_11
- 특허 번호
- US06962933B1
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