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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1062983생성일: 2026년 10월 26일

2-Methyl-4-(trimethylstannyl)pyridine → 5-Methyl-thiophene-2-carboxylic acid [4-methoxy-7-(2-methyl-pyridin-4-yl)-benzothiazol-2-yl]-amide

https://huagongshe.com/reaction/1062983

반응식

참여 물질

역할이름HCID투입량
반응물2-Methyl-4-(trimethylstannyl)pyridineHCID 12691320—
반응물5-Methyl-thiophene-2-carboxylic acid (4-methoxy-7-iodo-benzothiazol-2-yl)-amideHCID 86584906—
생성물5-Methyl-thiophene-2-carboxylic acid [4-methoxy-7-(2-methyl-pyridin-4-yl)-benzothiazol-2-yl]-amideHCID 1011131050%

반응 단계

5-Methyl-thiophene-2-carboxylic acid [4-methoxy-7-(2-methyl-pyridin-4-yl)-benzothiazol-2-yl]-amide is synthesized from 5-methyl-thiophene-2-carboxylic acid (4-methoxy-7-iodo-benzothiazol-2-yl)-amide (260 mg, 0.60 mmol) and 2-methyl-4-trimethylstannanyl-pyridine (384 mg, 0.90 mmol) using the general procedure B as a light yellow solid in 50% yield. MS: m/e=396 (M+H+).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06963000B2
출처 데이터셋uspto-grants-2005_11
ORD IDord-0c985697a2a3430c87e858c8c521131d
출처 메모uspto-grants-2005_11