Methyl atropate → Methyl phenylglyoxalate

HRID 1065740

반응식

HRID 1065740 반응식
[C:1]([O:11][CH3:12])(=[O:10])[C:2]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=C.C(O)(=[O:31])CCCCCCC/C=C\CCCCCCCC>C(O)(=O)C>[C:2]([C:1]([O:11][CH3:12])=[O:10])(=[O:31])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

참가 물질

4

반응물 2

HCID 193334Methyl atropateHCID 445639Oleic Acid

생성물 1

HCID 84835Methyl phenylglyoxalate수율 88%

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

The co-oxidation reaction was carried out in manner as described in Example 16, except that methyl atropate was used in lieu of oleic acid. As a result, acetic acid was obtained at a yield of 95% and methyl benzoylformate was obtained at a yield of 88%.

후처리

  1. customThe co-oxidation reaction

출처 및 근거

ORD 기록
ord-cba2002bf722486e97dfbc4f4ed88723
출처 데이터셋
uspto-grants-1982_05
특허 번호
US04331608

연결된 노트

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