Hydrochloric Acid → 1-Aminohexan-2-one hydrochloride

HRID 1065766노트

반응식

HRID 1065766 반응식
C([NH:4][CH:5]([C:11](=[O:16])[CH2:12][CH2:13][CH2:14][CH3:15])C(OCC)=O)(=O)C.[ClH:17]>>[ClH:17].[NH2:4][CH2:5][C:11](=[O:16])[CH2:12][CH2:13][CH2:14][CH3:15]

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 23325041HCID 23325041, 화합물

생성물 1

HCID 233250431-Aminohexan-2-one hydrochloride

실험 절차

Ethyl 2-acetamido-3-oxoheptanoate (10.4 g) was hydrolysed by heating under reflux with 50% hydrochloric acid (80 ml) for 9 hours. The mixture was evaporated to dryness to give 1-amino-2-hexanone hydrochloride (5.8 g) as a dark red oil.

후처리

  1. temperatureby heating
  2. customThe mixture was evaporated to dryness

출처 및 근거

ORD 기록
ord-cd576317dc324b56a01f9e657663c6b7
출처 데이터셋
uspto-grants-1982_05
특허 번호
US04331668

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