4-Ethoxybenzoic acid → 3-BROMO-4-ETHOXYBENZOIC ACID
반응식
[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][C:7]([C:8]([OH:10])=[O:9])=[CH:6][CH:5]=1)[CH3:2].[Br:13]Br>C(Cl)(Cl)Cl>[Br:13][C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:4]=1[O:3][CH2:1][CH3:2])[C:8]([OH:10])=[O:9]참가 물질
4
실험 절차
To a solution of 4ethoxybenzoic acid (3.6 g, 0.022 mol) in chloroform (60 ml) was added bromine (1.13 ml, 0.022 mol) in chloroform (20 ml) dropwise. After stirring overnight at room temperature the precipitate was filtered off and dried to afford the title compound as a white solid.
후처리
- filtrationwas filtered off
- customdried
출처 및 근거
- ORD 기록
- ord-f98146b56e02444fa978c9f341886fd9
- 출처 데이터셋
- uspto-grants-2001_06
- 특허 번호
- US06248754B1
반응 노트
불러오는 중…