Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-chloro-N-ethylbenzamide → n-Ethyl-2-chloro-6-(ethenyldimethylsilyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| 반응물 | Chloro(dimethyl)vinylsilane | HCID 519368 | — |
| 생성물 | n-Ethyl-2-chloro-6-(ethenyldimethylsilyl)benzamide | HCID 18630374 | — |
반응 단계
The title compound was prepared from the compound of Example f and 1.5 eq vinyldimethylsilyl chloride according to General Method C. Purification by HPLC with 1:4 ethyl acetate/hexanes gave 630 mg of the desired product as a white solid, a 9% yield. m.p. 86-89° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06248894B1 |
| 출처 데이터셋 | uspto-grants-2001_06 |
| ORD ID | ord-d92c24af9b2a4212b69d6542ac3da283 |
| 출처 메모 | uspto-grants-2001_06 |