HRID1068295

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID347962

2-chloro-N-ethylbenzamide

C9H10ClNO

HCID519368

Chloro(dimethyl)vinylsilane

C4H9ClSi

PRODUCTS

生成物

HCID18630374

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from the compound of Example f and 1.5 eq vinyldimethylsilyl chloride according to General Method C. Purification by HPLC with 1:4 ethyl acetate/hexanes gave 630 mg of the desired product as a white solid, a 9% yield. m.p. 86-89° C.

WORKUP

后处理

customPurification by HPLC with 1:4 ethyl acetate/hexanes