Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1073460생성일: 2026년 10월 27일
1-O-hexadecyl-2-O-methylglycerol → 3-(Hexadecyloxy)-2-methoxypropyl phenyl phosphorochloridate
https://huagongshe.com/reaction/1073460
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-O-hexadecyl-2-O-methylglycerol | HCID 1380 | — |
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | Phosphorodichloridic acid, phenyl ester | HCID 13038 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 3-(Hexadecyloxy)-2-methoxypropyl phenyl phosphorochloridate | HCID 22158627 | — |
반응 단계
A 1 mmol portion of 3-(hexadecyloxy)-2-methoxy propanol is added to a 0°-5° C. solution of 1 mmol of phenyl dichlorophosphate in 2 ml of anhydrous dichloromethane containing 1.2 mmol of triethylamine. The mixture is stirred under argon for 1 hour at 5° C., then for 2.5 hours at room temperature and then used as is.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04968790 |
|---|
| 출처 데이터셋 | uspto-grants-1990_11 |
|---|
| ORD ID | ord-2c6ff3b38cb74657812fe94e3396e1f8 |
|---|
| 출처 메모 | uspto-grants-1990_11 |
|---|
