反应详情

温度

5 °C

A 1 mmol portion of 3-(hexadecyloxy)-2-methoxy propanol is added to a 0°-5° C. solution of 1 mmol of phenyl dichlorophosphate in 2 ml of anhydrous dichloromethane containing 1.2 mmol of triethylamine. The mixture is stirred under argon for 1 hour at 5° C., then for 2.5 hours at room temperature and then used as is.

1. waitfor 2.5 hours at room temperature