Sodium hydride → HCID 14988300, 화합물

반응식

[N:1]1[CH:6]=[CH:5][C:4]([NH:7][N:8]2[C:16]3[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=3)[CH:10]=[CH:9]2)=[CH:3][CH:2]=1.[CH3:17][N:18]([CH2:20][CH2:21][CH2:22]Cl)[CH3:19].[H-].[Na+]>>[CH3:17][N:18]([CH2:20][CH2:21][CH2:22][N:7]([C:4]1[CH:3]=[CH:2][N:1]=[CH:6][CH:5]=1)[N:8]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:10]=[CH:9]1)[CH3:19]

참가 물질

반응물 3

HCID 24758Sodium hydride

HCID 669603-Chloro-N,N-dimethyl-1-propanamine

HCID 3081186N-(4-pyridinyl)-1H-indol-1-amine

생성물 1

HCID 14988300HCID 14988300, 화합물

실험 절차

The title compound was prepared from N-(4-pyridinyl)-1H-indol-1-amine and dimethylaminopropyl chloride with the aid of NaH in substantially the same manner as in Example 4. The product was obtained as an oil.

후처리

customThe product was obtained as an oil

출처 및 근거

ORD 기록: ord-730c8faaf4ad4919b3d114cecf123181
출처 데이터셋: uspto-grants-1990_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04970218

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