참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-Methyl-1-butene | HCID 11239 | — |
| 반응물 | Hexafluoroacetone | HCID 12695 | — |
| 생성물 | 5-Hydroxy-2-methyl-6,6,6-trifluoro-5-trifluoromethylhex-2-ene | HCID 12783437 | — |
반응 단계
A stirred mixture of hexafluoroacetone (235 g) and 3-methylbut-1-ene (100 g) was heated at 125° C. under a pressure of 17 atmospheres for a period of 20 hours. Distillation of the product mixture under reduced pressure yielded 5-hydroxy-2-methyl-6,6,6-trifluoro-5-trifluoromethylhex-2-ene as a mobile colorless liquid, b.p. 43° C./ 15 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04970330 |
|---|
| 출처 데이터셋 | uspto-grants-1990_11 |
|---|
| ORD ID | ord-3db4a1e00c554df59c627d5af31c15de |
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| 출처 메모 | uspto-grants-1990_11 |
|---|
