Hydrochloric Acid → HCID 22155954, 화합물

HRID 1074199노트

반응식

HRID 1074199 반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][C:11]2[NH:12][CH:13]=[CH:14][N:15]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[ClH:16]>CO.C(O)C>[ClH:16].[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][C:11]2[NH:15][CH:14]=[CH:13][N:12]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2]

참가 물질

5

반응물 2

HCID 313Hydrochloric AcidHCID 150774982-[(4-Nitrophenyl)thio]-1H-imidazole

생성물 1

HCID 22155954HCID 22155954, 화합물

시약·촉매·용매 2

HCID 702Ethanol용매HCID 887Methanol용매

실험 절차

The product from Example 26 was dissolved in methanol and treated with an excess of hydrogen chloride in ethyl alcohol. The mixture was concentrated and the residue triturated with ether and filtered. The solid was recrystallized from methanol to give the product as colorless prisms, mp 235°-240° C. (sealed tube).

후처리

  1. concentrationThe mixture was concentrated
  2. customthe residue triturated with ether
  3. filtrationfiltered
  4. customThe solid was recrystallized from methanol
  5. customto give

출처 및 근거

ORD 기록
ord-02409625d3164c6985dedd1c1d7c52dc
출처 데이터셋
uspto-grants-1990_11
특허 번호
US04973599

반응 노트

불러오는 중…