Endralazine → HCID 12582661, 화합물

HRID 1075936노트

반응식

HRID 1075936 반응식
[C:1]([N:9]1[CH2:20][CH2:19][C:12]2[N:13]=[N:14][C:15]([NH:17][NH2:18])=[CH:16][C:11]=2[CH2:10]1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C1(=O)CCCCC1>[C:1]([N:9]1[CH2:20][CH2:19][C:12]2[N:13]=[N:14][C:15]([NH:17][N:18]=[C:2]3[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]3)=[CH:16][C:11]=2[CH2:10]1)(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

3

반응물 1

HCID 47608Endralazine

생성물 1

HCID 12582661HCID 12582661, 화합물

시약·촉매·용매 1

HCID 7967Cyclohexanone용매

실험 절차

A suspension of 8.3 g of 6-benzoyl-3-hydrazino-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine in 20 cc of cyclohexanone is boiled at reflux at a bath temperature of 180° for 2 hours. The title compound has a M.P. of 188°-191° (decomp., from acetonitrile).

후처리

  1. temperatureat reflux at a bath temperature of 180° for 2 hours

출처 및 근거

ORD 기록
ord-cd171e03859a4f06be5a85d3e678e994
출처 데이터셋
uspto-grants-1976_05
특허 번호
US03954754

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