Phosphorus sulfide (P2S5) → HCID 21539496, 화합물

HRID 1076241노트

반응식

HRID 1076241 반응식
[C:1]1([C:7]2([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=3)[CH2:12][NH:11][CH2:10][NH:9][C:8]2=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.P12(SP3(SP(SP(S3)(S1)=S)(=S)S2)=S)=[S:21]>>[C:1]1([C:7]2([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=3)[CH2:12][NH:11][CH2:10][NH:9][C:8]2=[S:21])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 14817Phosphorus sulfide (P2S5)HCID 215394771,2,3,6-tetrahydro-5-phenyl-5-(2-pyridyl)-4(5H)-pyrimidinone

생성물 1

HCID 21539496HCID 21539496, 화합물

실험 절차

Treatment of 1,2,3,6-tetrahydro-5-phenyl-5-(2-pyridyl)-4(5H)-pyrimidinone with phosphorus pentasulfide as described in the procedure of Example 1 gives 1,2,3,6-tetrahydro-5-phenyl-5(2-pyridyl)-4(5H)-pyrimidinethione.

출처 및 근거

ORD 기록
ord-79a8e8ece5b84344b26e6d60a1f55f63
출처 데이터셋
uspto-grants-1976_05
특허 번호
US03956325

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