돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1077488생성일: 2026년 10월 25일

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3-dimethyl-4-methoxyphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/1077488

반응식

참여 물질

역할이름HCID투입량
반응물5,6-Diamino-1,3-dimethyluracilHCID 79501—
반응물4-Methoxy-2,3-dimethylcinnamic acidHCID 53401770—
생성물1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3-dimethyl-4-methoxyphenyl)ethenyl)-, (E)-HCID 644886522%

반응 단계

Substantially the same procedure as in Reference Example 70 was repeated using 1.74 g (10.2 mmol) of 5,6-diamino-1,3-dimethyluracil and 2.42 g (11.8 mmol) of 4-methoxy-2,3-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from acetonitrile to give 750 mg (yield 22%) of Compound 93 as a white powder.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05543415
출처 데이터셋uspto-grants-1996_08
ORD IDord-8bda6e765cd74330836d126ed4c23b07
출처 메모uspto-grants-1996_08