Hydrochloric Acid → HCID 14795572, 화합물

HRID 1084782노트

반응식

HRID 1084782 반응식
Cl.[C:2]([NH:6][CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)([CH3:5])([CH3:4])[CH3:3].[N:13]([O-])=[O:14].[Na+]>O>[N:13]([N:6]([C:2]([CH3:5])([CH3:3])[CH3:4])[CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)=[O:14]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 103920N-tert-ButylcyclohexylamineHCID 23668193Sodium Nitrite

생성물 1

HCID 14795572HCID 14795572, 화합물

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
90 °C

실험 절차

A mixture consisting of 13.2 ml of 10N hydrochloric acid, 50 ml of water, 18.8 g of tert.-butyl-cyclohexyl-amine and 17.9 g of sodium nitrite is heated at 90° C. for 3 hours. On cooling, a solid precipitates and is filtered off with suction. Yield: 16.3 g melting point: 87° C.

후처리

  1. temperatureOn cooling
  2. customa solid precipitates
  3. filtrationis filtered off with suction

출처 및 근거

ORD 기록
ord-77aa9f8eb74141e79be38cc3de5af618
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05006540

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