Triethylamine → HCID 86744708, 화합물

HRID 1084800

반응식

HRID 1084800 반응식
[CH:1](=[N:6][OH:7])[C:2]([CH3:5])([CH3:4])[CH3:3].ClN1C(=O)CCC1=O.[CH:16]([P:18](=[O:25])([O:22][CH2:23][CH3:24])[O:19][CH2:20][CH3:21])=[CH2:17].C(N(CC)CC)C>ClCCl.N1C=CC=CC=1>[C:2]([C:1]1[CH2:17][CH:16]([P:18](=[O:25])([O:22][CH2:23][CH3:24])[O:19][CH2:20][CH3:21])[O:7][N:6]=1)([CH3:5])([CH3:4])[CH3:3]

참가 물질

7

반응물 4

HCID 8471TriethylamineHCID 31398ChlorosuccinimideHCID 69629Diethyl vinylphosphonateHCID 136457Pivalaldoxime

생성물 1

HCID 86744708HCID 86744708, 화합물

시약·촉매·용매 2

HCID 1049Pyridine용매HCID 6344Dichloromethane용매

실험 절차

The procedure is analogous to that of Example 25 using 15.2 g (0.15 mol) of pivalaldoxime, 22.0 g (0.165 mol) of N-chlorosuccinimide, 0.5 ml of pyridine, 27.1 g (0.165 mol) of diethyl vinylphosphonate and 22.9 ml (0.165 mol) of triethylamine in dichloromethane. The product is obtained as an oil after the usual working up.

후처리

  1. customThe product is obtained as an oil after the

출처 및 근거

ORD 기록
ord-f7ff29b72e2e4375b1d0bcfc664d7b01
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05006515

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