p-Fluoronitrobenzene → HCID 21625360, 화합물

HRID 1085265

반응식

HRID 1085265 반응식
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH3:11][NH:12][CH2:13][CH2:14][N:15]([CH3:20])[CH2:16][CH2:17][NH:18][CH3:19]>CS(C)=O>[CH3:11][N:12]([C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1)[CH2:13][CH2:14][N:15]([CH3:20])[CH2:16][CH2:17][NH:18][CH3:19]

참가 물질

4

반응물 2

HCID 9590p-FluoronitrobenzeneHCID 669301,4,7-Trimethyldiethylenetriamine

생성물 1

HCID 21625360HCID 21625360, 화합물

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

반응 조건

온도
120 °C

실험 절차

In 7 ml of dimethyl sulfoxide were dissolved 1.41 g of p-fluoronitrobenzene and 14 g of N,N',N"-trimethyldiethylenetriamine, and the mixture was then stirred at 120° C. for 3 hours.

출처 및 근거

ORD 기록
ord-ea800a3811824a62a5c3612ba298168a
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05008267

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