Hydrazine hydrate (1:1) → HCID 20060099, 화합물

HRID 1085465노트

반응식

HRID 1085465 반응식
Cl[C:2]1[N:7]=[C:6]([CH3:8])[CH:5]=[C:4]([CH:9]2[CH2:11][CH2:10]2)[N:3]=1.O.[NH2:13][NH2:14]>C(O)C>[NH:13]([C:2]1[N:7]=[C:6]([CH3:8])[CH:5]=[C:4]([CH:9]2[CH2:11][CH2:10]2)[N:3]=1)[NH2:14]

참가 물질

4

반응물 2

HCID 24654Hydrazine hydrate (1:1)HCID 19804698HCID 19804698, 화합물

생성물 1

HCID 20060099HCID 20060099, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

3.0 g of 2-chloro-4-methyl-6-cyclopropylpyrimidine are dissolved in 30 ml of ethanol; 3.8 ml of hydrazine hydrate are added and the mixture is stirred for 20 hours at room temperature. The solvent is then evaporated off in vacuo and the residue is recrystallised with ethyl acetate. M.p. 98°-99° C.

후처리

  1. customThe solvent is then evaporated off in vacuo
  2. customthe residue is recrystallised with ethyl acetate

출처 및 근거

ORD 기록
ord-80d05987f4c04b3f87a30da479f6ac04
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05010082

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