Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4,5-Trimethoxybenzoyl chloride → N-(2,4,5-Trimethoxybenzoyl)-2-bromopyrrole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4,5-Trimethoxybenzoyl chloride | HCID 2760809 | — |
| 반응물 | 2-Bromopyrrole | HCID 12235268 | — |
| 생성물 | N-(2,4,5-Trimethoxybenzoyl)-2-bromopyrrole | HCID 18788308 | 55.1% |
반응 단계
Following the procedure for Example B, 2,4,5-trimethoxybenzoyl chloride (1.38 g, 6 mmol) and 2-bromopyrrole (4 mmol) gave 0.75 g of the title compound: mp 120-121° C.; 1H NMR (CDCl3) δ: 7.05-6.95 (2 H, m), 6.52 (1 H, s), 6.35 (1 H, dd, J=3.3, 1.8), 6.18 (1 H, t, J=3.5), 3.96 (3 H, s), 3.86 (3 H, s), 3.76 (3 H, s).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06057315 |
| 출처 데이터셋 | uspto-grants-2000_05 |
| ORD ID | ord-94d669171bd14385845297a4523e4dd4 |
| 출처 메모 | uspto-grants-2000_05 |