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Palmitoyl chloride → HCID 136341911, 화합물

HRID 1107413
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HRID 1107413 반응식
[C:1]([C@@:18]1([N:26]2[C:36]3[N:35]=[C:33]([NH2:34])[NH:32][C:30](=[O:31])[C:29]=3[N:28]=[CH:27]2)[O:25][C@H:22]([CH2:23][OH:24])[C@@H:20]([OH:21])[CH2:19]1)(=[O:17])[CH2:2][CH2:3][CH2:4]CCCCCCCCCCCC.C(Cl)(=O)CCC.C(Cl)(=O)CCCCCCCCCCCCCCC>>[C:1]([C@@:18]1([N:26]2[C:36]3[N:35]=[C:33]([NH2:34])[NH:32][C:30](=[O:31])[C:29]=3[N:28]=[CH:27]2)[O:25][C@H:22]([CH2:23][OH:24])[C@@H:20]([OH:21])[CH2:19]1)(=[O:17])[CH2:2][CH2:3][CH3:4]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 3

HCID 8206Palmitoyl chlorideHCID 8855Butyryl chlorideHCID 136333583HCID 136333583, 화합물

생성물 1

HCID 136341911HCID 136341911, 화합물

실험 절차

This compound was prepared using the procedure for palmitoyl-2'-deoxyguanosine, substituting the appropriate amount of butyryl chloride for palmitoyl chloride, and isolating as follows: evaporating the solvent after 72 hours, triturating the resulting material in 1:1 diethyl ether-ethyl acetate, and recovering the product by filtration.

후처리

  1. customThis compound was prepared
  2. customisolating
  3. customevaporating the solvent after 72 hours
  • customtriturating the resulting material in 1:1 diethyl ether-ethyl acetate
  • customrecovering the product
  • filtrationby filtration
  • 출처 및 근거

    ORD 기록
    ord-bddf4f15dc2042b7a194ce9ccf3fc429
    출처 데이터셋
    uspto-grants-2000_05
    DOI
    10.6084/m9.figshare.5104873.v1
    특허 번호
    US06060459

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