홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

tert-Butyl bromoacetate → 1-[(tert-Butoxycarbonyl)methyl]-Nalpha-benzyloxycarbonyl-D-tryptophan

HRID 1108206
노트
인쇄 미리보기

반응식

HRID 1108206 반응식
C[Si]([N-][Si](C)(C)C)(C)C.[Na+].[CH2:11]([O:18][C:19]([NH:21][C@@H:22]([C:33]([OH:35])=[O:34])[CH2:23][C:24]1[C:32]2[C:27](=[CH:28][CH:29]=[CH:30][CH:31]=2)[NH:26][CH:25]=1)=[O:20])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.Br[CH2:37][C:38]([O:40][C:41]([CH3:44])([CH3:43])[CH3:42])=[O:39]>O1CCCC1>[C:41]([O:40][C:38]([CH2:37][N:26]1[C:27]2[C:32](=[CH:31][CH:30]=[CH:29][CH:28]=2)[C:24]([CH2:23][C@H:22]([C:33]([OH:35])=[O:34])[NH:21][C:19]([O:18][CH2:11][C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[O:20])=[CH:25]1)=[O:39])([CH3:44])([CH3:43])[CH3:42]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 79177tert-Butyl bromoacetateHCID 700663N-(Benzyloxycarbonyl)-D-tryptophanHCID 2724254Sodium bis(trimethylsilyl)amide

생성물 1

HCID 538032101-[(tert-Butoxycarbonyl)methyl]-Nalpha-benzyloxycarbonyl-D-tryptophan수율 101.7%

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매3회

실험 절차

600 ml of a solution of NaHMDS (sodium salt of 1,1,1,3,3,3-hexamethyldisilazane) (1M) in tetrahydrofuran are added dropwise, at -78° C. under an inert atmosphere, to a solution of 100 g of Nα-benzyloxycarbonyl-D-tryptophan in a liter of anhydrous tetrahydrofuran. After one hour, the temperature is brought to 0° C. and a solution of 64 g of tert-butyl bromoacetate in 50 ml of anhydrous tetrahydrofuran is added dropwise. The reaction mixture is then brought to ambient temperature and the solvent is subsequently evaporated off in vacuo. The residue is diluted with dichloromethane and the solution is acidified by adding an aqueous 4N hydrochloric acid solution. After extraction with dichloromethane, the organic phases are dried over sodium sulphate and then concentrated in vacuo. 136 g of the expected product are obtained.

후처리

  1. customis brought to 0° C.
  2. customis then brought to ambient temperature
  3. customthe solvent is subsequently evaporated off in vacuo
  4. additionThe residue is diluted with dichloromethane
  5. additionby adding an aqueous 4N hydrochloric acid solution
  6. extractionAfter extraction with dichloromethane
  7. dry with materialthe organic phases are dried over sodium sulphate
  8. concentrationconcentrated in vacuo

출처 및 근거

ORD 기록
ord-858fd614e1bd497186f9d18efd6ddb17
출처 데이터셋
uspto-grants-2000_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06066633

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트