Ethyl α-(acetylamino)-6-quinolinepropanoate → HCID 21925070, 화합물

HRID 1108498노트

반응식

HRID 1108498 반응식
C([O:3][C:4](=[O:21])[CH:5]([CH2:10][C:11]1[CH:12]=[C:13]2[C:18](=[CH:19][CH:20]=1)[N:17]=[CH:16][CH:15]=[CH:14]2)[NH:6]C(=O)C)C>Cl>[N:17]1[C:18]2[C:13](=[CH:12][C:11]([CH2:10][CH:5]([C:4]([OH:21])=[O:3])[NH2:6])=[CH:20][CH:19]=2)[CH:14]=[CH:15][CH:16]=1

참가 물질

3

반응물 1

HCID 21925091Ethyl α-(acetylamino)-6-quinolinepropanoate

생성물 1

HCID 21925070HCID 21925070, 화합물

시약·촉매·용매 1

HCID 313Hydrochloric Acid용매

실험 절차

N-Acetyl β-(6-quinolinyl)-D,L-alanine ethyl ester (728 mg, 2.55 mmol) was heated at reflux in 6 N HCl (20 mL). After 20 h, the reaction mixture was concentrated to dryness and the residue was dried in vacuo to provide the title compound, which was used directly in next reaction.

후처리

  1. concentrationthe reaction mixture was concentrated to dryness
  2. customthe residue was dried in vacuo

출처 및 근거

ORD 기록
ord-f8ef375953254f27b60e8393ddd7a19e
출처 데이터셋
uspto-grants-2000_05
특허 번호
US06066730

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